The second Phyllis Coates's scene as the fabulous damsel Lois Lane occurrs in the sixth episode where Lois is captured in a motel together with the wife of the murdered motel owner. While his murderers are waiting for some other killer to come and get rid of the ladies (yeah stupid plot but thanks to it we have this scene so I am not complaining).
The ladies are tied back to back and OTM gagged. Unfortunately we don't see the other woman's (Ann Doran) face. They are untied by Jimmy who is mistakem for the other killer.